HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-5-nitrobenzoic acid → HCID 59313931, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-5-nitrobenzoic acid | HCID 239336 | — |
| Reactant | HCID 12104633 | HCID 12104633 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59313931 | HCID 59313931 | — |
Reaction Steps
3-Nitro-5-(1H-1,2,4-triazol-1-yl)benzoic acid was prepared from 3-bromo-5-nitrobenzoic acid following the procedure in Intermediate 2A. HPLC: Rt=1.12 min. (PHENOMENEX® Luna 5 micron C18 4.6×30 mm, 10-90% aqueous methanol containing 0.1% TFA, 2 min. gradient, flow rate=5 mL/min., detection at 254 nm). MS (ES): m/z=235.07 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252795B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-5a8b851b93fe4a93a708f19be2772e7d |
| Source note | uspto-grants-2012_08 |