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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 889620Generated: November 1, 2026

6-Bromohexanoic acid → HCID 178433620, compound

https://huagongshe.com/reaction/889620

Reaction equation

Participants

RoleNameHCIDCharge
Reactant6-Bromohexanoic acidHCID 20210—
Reactant2,3,3-Trimethyl-3H-pyrrolo[2,3-b]pyridineHCID 22266836—
SolventEthyl AcetateHCID 8857—
ProductHCID 178433620HCID 178433620—

Reaction Conditions

Temperature120 °C

Reaction Steps

A mixture of 0.54 g of 2,3,3-trimethyl-3H-pyrrolo[2,3-b]pyridine and 1.32 g of 6-bromohexanoic acid is heated at 120° C. for one hour. Ethyl acetate (10 mL) is added, and the reaction mixture is heated at reflux for 15 minutes, then cooled to room temperature. The supernatant liquid is decanted to yield the product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08252932B2
Source datasetuspto-grants-2012_08
ORD IDord-6cc9718c5011484c98a5c1caada89780
Source noteuspto-grants-2012_08