HCID 22248789, compound → HCID 22248797, compound

HRID 889824Notes

Reaction equation

HRID 889824 reaction equation
[CH2:1]([N:6]1[C:11](=[O:12])[NH:10][CH:9](OC)[C:8]([C:15]2[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][CH:16]=2)=[N:7]1)[CH2:2][CH2:3][CH2:4][CH3:5]>C1(C)C=CC=CC=1>[CH2:1]([N:6]1[C:11](=[O:12])[N:10]=[CH:9][C:8]([C:15]2[CH:16]=[CH:17][C:18]([Cl:21])=[CH:19][CH:20]=2)=[N:7]1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 1

HCID 22248789HCID 22248789, compound

Product 1

HCID 22248797HCID 22248797, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

A 0.5 g sample of 2-pentyl-5-methoxy-6-(4-chlorophenyl)-4,5-dihydro-1,2,4-triazin-3-one was dissolved in toluene. The toluene was removed from the product by distillation at atmospheric pressure to give 0.28 g of 2-pentyl-6-(4-chlorophenyl)-1,2,4-triazin-3-one (Compound 2).

Workup

  1. customThe toluene was removed from the product by distillation at atmospheric pressure

Sources & evidence

ORD record
ord-b33815de949c46f8bb967e8e697a0b3d
Source dataset
uspto-grants-2006_02
Patent number
US06995157B2

Reaction notes

Loading…