HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride → 2-(Tritylthio)ethylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride | HCID 6356 | — |
| Reactant | Triphenylcarbinol | HCID 6457 | — |
| Reactant | Cysteamine Hydrochloride | HCID 9082 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-(Tritylthio)ethylamine hydrochloride | HCID 18427267 | — |
Reaction Steps
1 equivalent of cysteamine hydrochloride and 1 equivalent of triphenylmethanol are dissolved in glacial acetic acid at 60° and treated with stirring with 1.1 equivalents of BF3 etherate. The mixture is stirred for one hour and worked up in the customary manner and Trt-cysteamine hydrochloride (“C”) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06995238B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-22221f657b7742bebbb0ac2716046337 |
| Source note | uspto-grants-2006_02 |