HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Phosphate, Tribasic → HCID 86597783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Phosphate, Tribasic | HCID 62657 | — |
| Reactant | 4-(Trifluoromethoxy)phenylboronic acid | HCID 2734386 | — |
| Reactant | Methyl 6-chloro-4-(trifluoromethyl)nicotinate | HCID 2775340 | — |
| Catalyst | Dichlorobis(triphenylphosphine)palladium | HCID 6102075 | — |
| Product | HCID 86597783 | HCID 86597783 | — |
Reaction Steps
In analogy to the procedure described in example 13 a], 4-(trifluoromethoxy)-phenylboronic acid was reacted with methyl 6-chloro-4-(trifluoromethyl)nicotinate in the presence of bis(triphenylphosphine)palladium(II)chloride and aqueous 2M K3PO4 solution to give the title compound as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06995263B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-f88a05de506c46b5a09aac9a0d990ab1 |
| Source note | uspto-grants-2006_02 |