HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 890848Generated: October 29, 2026
N-Benzylideneaniline → 1-Propanamine, N-(phenylmethylene)-3-(trimethoxysilyl)-
https://huagongshe.com/reaction/890848
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | N-Benzylideneaniline | HCID 10858 | — |
| Reactant | Silane | HCID 23953 | — |
| Reactant | Aminopropyltrimethoxysilane | HCID 83756 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 1-Propanamine, N-(phenylmethylene)-3-(trimethoxysilyl)- | HCID 105543 | — |
Reaction Steps
25 grams (0.138 moles) of N-benzylidene aniline [cas no. 538-51-2, from TCI America] was combined with 24.7 grams (0.138 moles) of gamma-aminopropyltrimethoxysilane [cas no. 13822-56-5, Silquest A-1110 Silane from Crompton Corporation] and 100 grams of xylene. The resulting slurry was warmed to 90° C. for one hour before a vacuum of 20 mm Hg was applied. Distillation of the xylene and aniline resulted in 36 grams (98%) of N-benzylidene aminopropyltrimethoxysilane [cas no. 67674-55-9] by GC analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06998499B2 |
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| Source dataset | uspto-grants-2006_02 |
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| ORD ID | ord-f36fbff332df47769964876f6c3f4a53 |
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| Source note | uspto-grants-2006_02 |
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