HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → Ethanaminium, N,N,N-triethyl-2-hydroxy-, iodide (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Diethylethanolamine | HCID 7497 | — |
| Product | Ethanaminium, N,N,N-triethyl-2-hydroxy-, iodide (1:1) | HCID 80057 | 94.1% |
Reaction Steps
To 200 g of acetone, 117 g of N,N-diethylethanolamine and 116 g of iodomethane were dissolved. The solution was left for one day. The precipitated white solid was filtered off, and dispersed in 200 g of acetone again. The dispersion was filtered off, and dried to obtain 210 g of N,N,N-triethyl-N-(2-hydroxyethyl)ammonium iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001704B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-510d978d4d9e4f8885d2c37c31157d8a |
| Source note | uspto-grants-2006_02 |