3-Butylpentane-2,4-dione → HCID 22244645, compound

HRID 891066Notes

Reaction equation

HRID 891066 reaction equation
Cl.[NH:2]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][OH:12])=[CH:6][CH:5]=1)[NH2:3].[CH2:13]([CH:17]([C:21](=O)[CH3:22])[C:18](=O)[CH3:19])[CH2:14][CH2:15][CH3:16]>>[CH2:13]([C:17]1[C:18]([CH3:19])=[N:3][N:2]([C:4]2[CH:5]=[CH:6][C:7]([CH2:10][CH2:11][OH:12])=[CH:8][CH:9]=2)[C:21]=1[CH3:22])[CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 737633-Butylpentane-2,4-dioneHCID 222447112-(4-Hydrazinophenyl)ethanol hydrochloride

Product 1

HCID 22244645HCID 22244645, compound

Procedure

The title compound was prepared according to the procedure described in step 1 of Example 1 from 2-(4-hydrazinophenyl)ethanol hydrochloride and 3-n-butyl-2,4-pentanedione: MS (ESI) m/z 273 [M+H]+, 1H-NMR (CDCl3) δ 7.37-7.26 (4H, m), 3.87 (2H, t, J=6.8 Hz), 2.91 (2H, t, J=6.6 Hz), 2.39 (2H, t, J=7.6 Hz), 2.25 (3H, s), 2.22 (3H, s), 1.53-1.26 (4H, m), 0.94 (3H, t, J=7.1 Hz).

Sources & evidence

ORD record
ord-032491315a414c72abced4deddc4955c
Source dataset
uspto-grants-2006_02
Patent number
US07001917B2

Reaction notes

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