HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,5-Difluorophenyl)boronic acid → HCID 22244579, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,5-Difluorophenyl)boronic acid | HCID 2734338 | — |
| Reactant | 2-[4-(4-Iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol | HCID 22244559 | — |
| Product | HCID 22244579 | HCID 22244579 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 12 from 2-[4-(4-iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol (step 2 of Example 11) and 3,5-difluorobenzeneboronic acid: MS (ESI) m/z 329 [M+H]+, 1H-NMR (CDCl3) δ 7.70-7.63 (1H, m), 7.55-7.33 (4H, m), 6.87-6.73 (2H, m), 3.89 (2H, t, J=6.2 Hz), 2.93 (2H, t, J=6.6 Hz), 2.33 (3H, s), 2.30 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-6e85dcc7cfe54c9c9525a1dcebf1bcfd |
| Source note | uspto-grants-2006_02 |