4-Methoxybenzenesulfonamide → HCID 10311364, compound

HRID 891091Notes

Reaction equation

[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][NH:22][C:23](=O)[O:24]C3C=CC=CC=3)=[CH:16][CH:15]=2)[N:3]=1.[CH3:32][O:33][C:34]1[CH:39]=[CH:38][C:37]([S:40]([NH2:43])(=[O:42])=[O:41])=[CH:36][CH:35]=1>>[CH3:1][C:2]1[C:6]([C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][CH:12]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:15]=[CH:16][C:17]([CH2:20][CH2:21][NH:22][C:23]([NH:43][S:40]([C:37]3[CH:36]=[CH:35][C:34]([O:33][CH3:32])=[CH:39][CH:38]=3)(=[O:42])=[O:41])=[O:24])=[CH:18][CH:19]=2)[N:3]=1

Participants

Reactant 2

HCID 707894-Methoxybenzenesulfonamide

HCID 22244550Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate

Product 1

HCID 10311364HCID 10311364, compound

Procedure

The title compound was prepared according to the procedure described in step 2 of Example 22 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 4-(methyloxy)benzenesulfonamide: 1H-NMR (CDCl3) δ 7.77-7.73 (2H, m), 7.47-7.25 (9H, m), 6.96 (2H, d, J=9.1 Hz), 6.41 (1H, br.s), 3.85 (3H, s), 3.54-3.47 (2H, m), 2.87 (2H, t, J=6.7 Hz), 2.33 (3H, s), 2.27 (3H, s).

Sources & evidence

ORD record: ord-0a66866f144742e698244c808cb90b99
Source dataset: uspto-grants-2006_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07001917B2

Reaction notes

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