HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylbenzenesulfonamide → 4-tert-Butyl-N-[({2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylbenzenesulfonamide | HCID 222872 | — |
| Reactant | Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate | HCID 22244550 | — |
| Product | 4-tert-Butyl-N-[({2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]benzenesulfonamide | HCID 22244522 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 22 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 4-tert-butyl-benzenesulfonamide: 1H-NMR (CDCl3) δ 7.76 (2H, d, J=8.7 Hz), 7.53-7.24 (11H, m), 6.43 (1H, br.s), 3.54-3.47 (2H, m), 2.87 (2H, t, J=6.6 Hz), 2.33 (3H, s), 2.26 (3H, s), 1.32 (9H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-fab96d4332584b1389922162ca49931f |
| Source note | uspto-grants-2006_02 |