HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzenesulfonamide → N-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-4-fluorobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzenesulfonamide | HCID 120231 | — |
| Reactant | Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate | HCID 22244550 | — |
| Product | N-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-4-fluorobenzenesulfonamide | HCID 22244627 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 22 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 4-fluorobenzenesulfonamide: 1H-NMR (CDCl3) δ 7.94-7.88 (2H, m), 7.47-7.15 (11H, m), 6.24 (1H, br.s), 3.48-3.42 (2H, m), 2.84 (2H, t, J=7.0 Hz), 2.32 (3H, s), 2.23 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-a8909df293154eaba02331e291a941e8 |
| Source note | uspto-grants-2006_02 |