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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 891100Generated: October 25, 2026

m-Toluenesulphonamide → N-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-3-methylbenzenesulfonamide

https://huagongshe.com/reaction/891100

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-ToluenesulphonamideHCID 74697—
ReactantPhenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamateHCID 22244550—
ProductN-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-3-methylbenzenesulfonamideHCID 10217615—

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 22 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 3-methylbenzenesulfonamide: 1H-NMR (CDCl3) δ 7.72-7.66 (2H, m), 7.46-7.22 (11H, m), 6.45 (1H, br.s), 3.48-3.45 (2H, m), 2.86-2.81 (2H, m), 2.39 (3H, s), 2.32 (3H, s), 2.25 (3H, s).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07001917B2
Source datasetuspto-grants-2006_02
ORD IDord-60f0b5a1bc3c4e42b508bfa0f2dd7715
Source noteuspto-grants-2006_02