HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzene-1-sulfonamide → N-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-3-methoxybenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzene-1-sulfonamide | HCID 14763060 | — |
| Reactant | Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate | HCID 22244550 | — |
| Product | N-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-3-methoxybenzenesulfonamide | HCID 22244604 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 22 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 3-methoxybenzenesulfonamide: 1H-NMR (CDCl3) δ 7.47-7.09 (13H, m), 6.36 (1H, br.s), 3.81 (3H, s), 3.49-3.43 (2H, m), 2.83 (2H, t, J=6.6 Hz), 2.32 (3H, s), 2.24 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-c90cfed278734da4a723efa32bcdde57 |
| Source note | uspto-grants-2006_02 |