1,1,1-Trifluoro-2,4-pentanedione → HCID 22244551, compound

HRID 891117Notes

Reaction equation

HRID 891117 reaction equation
Cl.[NH:2]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][OH:12])=[CH:6][CH:5]=1)[NH2:3].[F:13][C:14]([F:22])([F:21])[C:15](=O)[CH2:16][C:17](=O)[CH3:18]>>[CH3:18][C:17]1[N:2]([C:4]2[CH:5]=[CH:6][C:7]([CH2:10][CH2:11][OH:12])=[CH:8][CH:9]=2)[N:3]=[C:15]([C:14]([F:22])([F:21])[F:13])[CH:16]=1

Participants

3

Reactant 2

HCID 739431,1,1-Trifluoro-2,4-pentanedioneHCID 222447112-(4-Hydrazinophenyl)ethanol hydrochloride

Product 1

HCID 22244551HCID 22244551, compound

Procedure

The title compound was prepared according to the procedure described in step 1 of Example 1 from 2-(4-hydrazinophenyl)ethanol hydrochloride and 1,1,1-trifluoro-2,4-pentanedione: MS (ESI) m/z 270 [M+H]+, 1H-NMR (CDCl3) δ 7.41-7.34 (4H, m), 6.45 (1H, s), 3.93-3.86 (211, m), 2.94 (2H, t, J=6.6 Hz), 2.34 (3H, s).

Sources & evidence

ORD record
ord-6d05ed0707c94b8ea8b7ea6759cb2b15
Source dataset
uspto-grants-2006_02
Patent number
US07001917B2

Reaction notes

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