1,3-Benzenedisulfonamide → HCID 22244643, compound

HRID 891124Notes

Reaction equation

HRID 891124 reaction equation
[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][NH:22][C:23](=[O:31])OC3C=CC=CC=3)=[CH:16][CH:15]=2)[N:3]=1.[C:32]1([S:42]([NH2:45])(=[O:44])=[O:43])[CH:37]=[CH:36][CH:35]=[C:34]([S:38]([NH2:41])(=[O:40])=[O:39])[CH:33]=1>>[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][NH:22][C:23]([NH:45][S:42]([C:32]3[CH:37]=[CH:36][CH:35]=[C:34]([S:38]([NH2:41])(=[O:40])=[O:39])[CH:33]=3)(=[O:44])=[O:43])=[O:31])=[CH:16][CH:15]=2)[N:3]=1

Participants

3

Reactant 2

HCID 30900441,3-BenzenedisulfonamideHCID 22244550Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate

Product 1

HCID 22244643HCID 22244643, compound

Procedure

The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 1,3-benzenedisulfonamide: 1H-NMR (CDCl3) δ 8.47 (1H, s), 8.05-7.95 (2H, m), 7.52-7.09 (10H, m), 6.27 (1H, br.s), 3.37-3.28 (2H, m), 2.75-2.64 (2H, m), 2.17 (3H, s), 2.13 (3H, s).

Sources & evidence

ORD record
ord-c418b7f9c3c2434c9616197ef0e5ac87
Source dataset
uspto-grants-2006_02
Patent number
US07001917B2

Reaction notes

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