Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate → HCID 22244537, compound

HRID 891140Notes

Reaction equation

HRID 891140 reaction equation
[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][NH:22][C:23](=O)[O:24]C3C=CC=CC=3)=[CH:16][CH:15]=2)[N:3]=1.[CH3:32][C:33]1[N:34]=[C:35]([S:39]([NH2:42])(=[O:41])=[O:40])[S:36][C:37]=1[CH3:38]>>[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:15]=[CH:16][C:17]([CH2:20][CH2:21][NH:22][C:23]([NH:42][S:39]([C:35]3[S:36][C:37]([CH3:38])=[C:33]([CH3:32])[N:34]=3)(=[O:40])=[O:41])=[O:24])=[CH:18][CH:19]=2)[N:3]=1

Participants

3

Reactant 2

HCID 22244550Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamateHCID 22244622HCID 22244622, compound

Product 1

HCID 22244537HCID 22244537, compound

Procedure

The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 4,5-dimethyl-1,3-thiazole-2-sulfonamide: 1H-NMR (CDCl3) δ 7.45-7.24 (9H, m), 6.47 (1H, br.s), 3.50-3.42 (2H, m), 2.88-2.82 (2H, m), 2.41 (3H, s), 2.35 (3H, s), 2.31 (3H, s), 2.24 (3H, s).

Sources & evidence

ORD record
ord-8cb06eafade34a6481e0e8ab7e2d56e6
Source dataset
uspto-grants-2006_02
Patent number
US07001917B2

Reaction notes

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