Dibenzoylmethane → HCID 22244635, compound

HRID 891158Notes

Reaction equation

HRID 891158 reaction equation
[C:1]1([C:7](=O)[CH2:8][C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[NH:19]([C:21]1[CH:26]=[CH:25][C:24]([CH2:27][CH2:28][OH:29])=[CH:23][CH:22]=1)[NH2:20]>>[C:1]1([C:7]2[CH:8]=[C:9]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=3)[N:19]([C:21]3[CH:22]=[CH:23][C:24]([CH2:27][CH2:28][OH:29])=[CH:25][CH:26]=3)[N:20]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 8433DibenzoylmethaneHCID 222447112-(4-Hydrazinophenyl)ethanol hydrochloride

Product 1

HCID 22244635HCID 22244635, compound

Procedure

The title compound was prepared according to the procedure described in step 1 of Example 1 from 1,3-diphenylpropane-1,3-dione and 2-(4-hydrazinophenyl)ethanol hydrochloride: MS (ESI) m/z 341 [M+H]+, 1H-NMR (CDCl3) δ 7.93-7.91 (2H, m), 7.46-7.20 (12H, m), 6.82 (1H, s), 3.87 (2H, br), 2.89 (2H, t, J=6.6 Hz).

Sources & evidence

ORD record
ord-907e8ba842d74181a6831882408681f8
Source dataset
uspto-grants-2006_02
Patent number
US07001917B2

Reaction notes

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