HCID 15711025, compound → HCID 22244688, compound

HRID 891159Notes

Reaction equation

HRID 891159 reaction equation
[CH:1]1([CH:7]([C:11](=O)[CH3:12])[C:8](=O)[CH3:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Cl.[NH:15]([C:17]1[CH:22]=[CH:21][C:20]([CH2:23][CH2:24][OH:25])=[CH:19][CH:18]=1)[NH2:16]>>[CH:1]1([C:7]2[C:11]([CH3:12])=[N:16][N:15]([C:17]3[CH:18]=[CH:19][C:20]([CH2:23][CH2:24][OH:25])=[CH:21][CH:22]=3)[C:8]=2[CH3:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 15711025HCID 15711025, compoundHCID 222447112-(4-Hydrazinophenyl)ethanol hydrochloride

Product 1

HCID 22244688HCID 22244688, compound

Procedure

The title compound was prepared according to the procedure described in step 1 of Example 1 from 3-cyclohexylpentane-2,4-dione (Tetrahedron, 1991, 47, 6511) and 2-(4-hydrazinophenyl)ethanol hydrochloride: 1H-NMR (CDCl3) δ 7.36-7.30 (4H, m), 391 (2H, t, J=6.6 Hz), 2.91 (2H, t, J=6.6 Hz), 2.31 (3H, s), 2.24 (3H, s), 1.82-1.26 (11H, m).

Sources & evidence

ORD record
ord-42014fcfbbfe4d4783d3b4ed362c7009
Source dataset
uspto-grants-2006_02
Patent number
US07001917B2

Reaction notes

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