HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexafluorophosphoric acid → HCID 178480861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexafluorophosphoric acid | HCID 16211447 | — |
| Reactant | HCID 178480860 | HCID 178480860 | — |
| Product | HCID 178480861 | HCID 178480861 | 78% |
Reaction Steps
1.2 equivalents of HPF6 were slowly added to 1-(3-phenylpropyl)-3-methylimidazolium chloride under ice cooling. After stirring for 30 minutes, the mixture was extracted with methylene chloride (MC) three times. The extract was dried over anhydrous sodium sulfate and concentrated to obtain 1-(3-phenylpropyl)3-methylimidazolium hexafluorophosphate (mp 52˜53° C., yield 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07005282B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-2a2e82447a66482a8bf66149237b0301 |
| Source note | uspto-grants-2006_02 |