HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178418806, compound → HCID 178503600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178418806 | HCID 178418806 | — |
| Reactant | HCID 178503599 | HCID 178503599 | — |
| Reactant | HCID 178517101 | HCID 178517101 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178503600 | HCID 178503600 | — |
Reaction Steps
The named compound is prepared by substituting 3-amino-5-methylsulfanyl-1H-pyrazole-4-carbonitrile for 3-aminopyrazole in the reaction of Example 1. Specifically, E & Z-3-[(hydroxy)-methylene]-1,3-dihydro-indol-2-one (0.100 gms.) is reacted with 0.2003 gms. of 3-amino-5-methylsulfanyl-1H-pyrazole-4-carbonitrile by refluxing in tetrahydrofuran (2.5 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07005444B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-27ce186adc1c490f902787e8109694b7 |
| Source note | uspto-grants-2006_02 |