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HRID892286

反应详情

EQUATION

反应方程式

HRID 892286 的结构方程式

REACTANTS

反应物

2
结构：NS(=O)(=O)c1cccc([N+](=O)[O-])c1
HCID67138

Benzenesulfonamide, 3-nitro-

C6H6N2O4S

结构：O=C(O)c1cc(Br)c(OCc2cccc(Br)c2)c(Br)c1
HCID22242280

未命名化合物

PRODUCTS

生成物

1
结构：O=C(NS(=O)(=O)c1cccc([N+](=O)[O-])c1)c1cc(Br)c(OCc2cccc(Br)c2)c(Br)c1
HCID10211644

未命名化合物

收率 54.4%

PROCEDURE

实验过程

3,5-dibromo-4-(3-bromobenzyloxy)benzoic acid (0.17 mmol) was coupled with 3-nitrobenzenesulphonamide (0.89 mmol) using the procedure described in Example 31. Purification on column (silica gel, chloroform/methanol 9:1) gave 60 mg (54%) of N-[3,5-dibromo-4-(3-bromobenzyloxy)benzoyl]-3-nitrobenzenesulphonamide.

WORKUP

后处理

  1. customPurification on column (silica gel, chloroform/methanol 9:1)