HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloropyridine → HCID 19895731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloropyridine | HCID 7977 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | 2-Phenylcyclohexanone | HCID 95592 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Reactant | HCID 19895730 | HCID 19895730 | — |
| Product | HCID 19895731 | HCID 19895731 | — |
Reaction Steps
The title compound was prepared from 2-phenyl-2-(2-pyridyl)-cyclohexanone (4.50 g, 0.017 mol, prepared from the alkylation of 2-phenylcyclohexanone with 2-chloropyridine and sodium hydride), 2,6-diisopropyl-phenyl isocyanate (3.60 g, 0.017 mol), and lithium diisopropylamide (0.017 mol) using the procedure described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118697 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-bc9646431ec742d99906ba83409e6f9b |
| Source note | uspto-grants-1992_06 |