HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diisopropylphenyl isocyanate → N-[2,6-bis(1-methylethyl)-phenyl]-2-oxo-3-(5-phenoxypentyl)-3-phenyl-cyclohexane carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Reactant | HCID 19895723 | HCID 19895723 | — |
| Product | N-[2,6-bis(1-methylethyl)-phenyl]-2-oxo-3-(5-phenoxypentyl)-3-phenyl-cyclohexane carboxamide | HCID 19895729 | — |
Reaction Steps
The title compound, mp 150°-153° C., was prepared from 2-(5-phenoxypentyl)-2-phenylcyclohexanone (2.50 g, 0.007 mol), 2,6 diisopropylphenyl isocyanate (1.42 g, 0.007 mol), and lithium diisopropylamide (0.007 mol) using the procedure described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118697 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-eb56117169c1462e87c318ba569cfe76 |
| Source note | uspto-grants-1992_06 |