HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19896092, compound → HCID 19896089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19896092 | HCID 19896092 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19896089 | HCID 19896089 | — |
Reaction Steps
Prepared according to the method described, starting from 13.0 g (0.06 mol) of PCC in 70 ml of CH2Cl2 and a solution of 6.45 g (0.038 mol) of 2,2,6-trimethyl-3-methylene-1-cyclohexanemethanol (obtained according to example 3a.) in 30 ml of CH2Cl2. After stirring for 2 h and treating as described, 5.58 g of a colorless oil, containing 80% of the desired aldehyde (2 isomers, cis/trans ~9:1) and a secondary product of no interest, were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118865 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-a7a3d9a51c4c40c78477a81ec2927be5 |
| Source note | uspto-grants-1992_06 |