Potassium Hydroxide → HCID 53986718, compound

HRID 892675Notes

Reaction equation

HRID 892675 reaction equation
[C:1]1([CH:7](Cl)[CH:8]([C:10]([F:13])([F:12])[F:11])[CH3:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[K+]>C(O)C>[C:1]1([CH:7]=[C:8]([C:10]([F:11])([F:12])[F:13])[CH3:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 19896130HCID 19896130, compound

Product 1

HCID 53986718HCID 53986718, compoundYield 71%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To 7 ml of ethanol added was 0.6 mmol (0.126 g) of 1-phenyl-1-chloro-2-trifluoromethylpropane, and then 2 mmol (0.112 g) of potassium hydroxide was added thereto and allowed to react at 50° C. for 18 hours, whereby 1-phenyl-2-trifluoromethylpropene was obtained at a yield of 71%. The results of analyses of the product are shown below.

Workup

  1. customto react at 50° C. for 18 hours

Sources & evidence

ORD record
ord-664e6ee2a23e447ca131408120f80e9d
Source dataset
uspto-grants-1992_06
Patent number
US05118879

Reaction notes

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