HuagongsheHuagongshe Chemistry Print Report · For research reference only
P,P'-dde → 1-Chloro-4-(2,2,2-trichloro-1-(4-chlorophenyl)ethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P,P'-dde | HCID 3035 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-Chloro-4-(2,2,2-trichloro-1-(4-chlorophenyl)ethyl)benzene | HCID 3036 | — |
Reaction Steps
Onto the p,p'-DDE obtained in Stage (b) 100 ml water is added, the mixture heated to 80° C.-85° C. and chlorine gas added over a period of 8-11 hours, until the concentration of p,p'-DDE drops to 0.2%. The upper aqueous phase is separated to afford 410 g p,p'-DDT, which was used directly in the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118881 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-8d9c2a7e776d4e9d912b4ad54aae4cc8 |
| Source note | uspto-grants-1992_06 |