HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 3767530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-(2,4-Dichlorophenyl)-2-furoic acid | HCID 776817 | — |
| Product | HCID 3767530 | HCID 3767530 | — |
Reaction Steps
A solution of 28.28 g (0.11 moles) of 5-(2,4-dichlorophenyl)-2-furancarboxylic acid in 43 ml of thionyl chloride is heated at reflux for 3 hours. The solvent is removed and the residue is treated with 100 ml of toluene. The solvent is removed and the residue is carried on directly to the next step of the reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118708 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-84d9ad6498b5485fa51c8890e8e06140 |
| Source note | uspto-grants-1992_06 |