HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylparaben → HCID 13972387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Homoallyl bromide | HCID 21241 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 13972387 | HCID 13972387 | — |
Reaction Steps
A slurry of 4-bromo-1-butene (1.4 g), methyl p-hydroxybenzoate (1.5 g) and K2CO3 (1.8 g) in acetone was heated to reflux for 18 hours. The reaction was cooled, filtered, and concentrated to a yellow oil. The oil was chromatographed with 20% ethyl acetate/hexanes to give the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05120729 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-0f35032e7b8f40f9a5e267b99d1ad594 |
| Source note | uspto-grants-1992_06 |