HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzaldehyde → 4-(3-Phenylpropylthio)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Reactant | 3-Phenylpropane-1-thiol | HCID 90596 | — |
| Product | 4-(3-Phenylpropylthio)benzaldehyde | HCID 19754542 | 101.2% |
Reaction Steps
By the method of Preparation 7, 3-phenylpropyl mercaptan (41.1 g) and 4-bromobenzaldehyde (53.7 g) were converted to 70 g of present title product, isolated as an oil following chromatography on silica gel using 9:1 hexane:ethyl acetate as eluant; tlc Rf 0.4 (1:4 ethyl acetate:hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05120754 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-2a239e00fcd44a16bc1c4c83cc215032 |
| Source note | uspto-grants-1992_06 |