M-Phenylenediamine → HCID 67793563, compound

HRID 892877Notes

Reaction equation

HRID 892877 reaction equation
[C:1]([OH:20])(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:21]1([NH2:28])[CH:26]=[CH:25][CH:24]=[C:23]([NH2:27])[CH:22]=1>>[C:1]([NH:27][C:23]1[CH:22]=[C:21]([CH:26]=[CH:25][CH:24]=1)[NH2:28])(=[O:20])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 7935M-PhenylenediamineHCID 445639Oleic Acid

Product 1

HCID 67793563HCID 67793563, compoundYield 70%

Procedure

Oleic acid (2.82 g) and m-phenylenediamine (1.62 g) were reacted in the same manner as Reference Example 11 to obtain 2.60 g of the objective compound (yield: 70%).

Sources & evidence

ORD record
ord-500bf1b73c244cec91fd32551118ceae
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

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