4-Aminothiophenol → HCID 86745896, compound

HRID 892880Notes

Reaction equation

[C:1]([OH:20])(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[NH2:21][C:22]1[CH:27]=[CH:26][C:25]([SH:28])=[CH:24][CH:23]=1>>[C:1](=[O:20])([S:28][C:25]1[CH:26]=[CH:27][C:22]([NH2:21])=[CH:23][CH:24]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

Reactant 2

HCID 145104-Aminothiophenol

HCID 445639Oleic Acid

Product 1

HCID 86745896HCID 86745896, compoundYield 74%

Procedure

Oleic acid (2.82 g) and 1.88 g of p-aminothiophenol were reacted in the same manner as in Reference Example 11 to obtain 2.86 g of the objective compound (yield: 74%).

Sources & evidence

ORD record: ord-96c5e8a8e4e948fbb6a08d87e873f1cd
Source dataset: uspto-grants-1992_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05120738

Reaction notes

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