1,2-Diaminocyclohexane, (+)- → HCID 67795427, compound

HRID 892886Notes

Reaction equation

HRID 892886 reaction equation
[NH2:1][C@H:2]1[CH2:7][CH2:6][CH2:5][CH2:4][C@@H:3]1[NH2:8].[C:9](OC)(=[O:27])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]/[CH:17]=[CH:18]\[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[C:9]([NH:1][C@H:2]1[CH2:7][CH2:6][CH2:5][CH2:4][C@@H:3]1[NH2:8])(=[O:27])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]/[CH:17]=[CH:18]\[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]

Participants

3

Reactant 2

HCID 4793071,2-Diaminocyclohexane, (+)-HCID 5364509Methyl Oleate

Product 1

HCID 67795427HCID 67795427, compoundYield 65%

Procedure

(S,S)-1,2-Diaminocyclohexane (1.14 g) and 2.96 g of methyl oleate were reacted in the same manner as in Reference Example 26 to obtain 2.41 g of the objective compound (yield: 65%)

Sources & evidence

ORD record
ord-ef32629f30bd4f899b7de2ed5d7ef92a
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

Loading…