HCID 16481601, compound → HCID 19893500, compound

HRID 892893Notes

Reaction equation

HRID 892893 reaction equation
[C:1]([NH:14][C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1)(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH3:22][C:23]1([CH3:39])[O:28][CH:27]([C:29]([NH:31][CH2:32][CH2:33][C:34](O)=[O:35])=[O:30])[C:26]([CH3:38])([CH3:37])[CH2:25][O:24]1>>[C:1]([NH:14][C:15]1[CH:21]=[CH:20][C:18]([NH:19][C:34](=[O:35])[CH2:33][CH2:32][NH:31][C:29]([CH:27]2[C:26]([CH3:37])([CH3:38])[CH2:25][O:24][C:23]([CH3:39])([CH3:22])[O:28]2)=[O:30])=[CH:17][CH:16]=1)(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 16481601HCID 16481601, compoundHCID 189385173-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid

Product 1

HCID 19893500HCID 19893500, compoundYield 83.3%

Procedure

4-Lauroylaminoaniline (250 mg) and 223 mg of 3-[N-(2,2,5,5-tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid were reacted in the same manner as in Example 1 to obtain 381 mg of the title compound (yield: 72%).

Sources & evidence

ORD record
ord-6d723928d34b4124b4e44a5361205b1a
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

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