HCID 19893582, compound → 4-(Oleoylamino)phenyl 3-[N-(2,4-diacetoxy-3,3-dimethyl-1-oxobutyl)amino]propionate

HRID 892895Notes

Reaction equation

[C:1]([NH:20][C:21]1[CH:26]=[CH:25][C:24]([OH:27])=[CH:23][CH:22]=1)(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:28]([O:31][CH:32]([C:41]([CH3:48])([CH3:47])[CH2:42][O:43][C:44](=[O:46])[CH3:45])[C:33]([NH:35][CH2:36][CH2:37][C:38](O)=[O:39])=[O:34])(=[O:30])[CH3:29]>>[C:28]([O:31][CH:32]([C:41]([CH3:48])([CH3:47])[CH2:42][O:43][C:44](=[O:46])[CH3:45])[C:33]([NH:35][CH2:36][CH2:37][C:38]([O:27][C:24]1[CH:25]=[CH:26][C:21]([NH:20][C:1](=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[CH:22][CH:23]=1)=[O:39])=[O:34])(=[O:30])[CH3:29]

Participants

Reactant 2

HCID 19893582HCID 19893582, compound

HCID 67633947p-Oleoylaminophenol

Product 1

HCID 677955914-(Oleoylamino)phenyl 3-[N-(2,4-diacetoxy-3,3-dimethyl-1-oxobutyl)amino]propionateYield 45.3%

Procedure

4-Oleoylaminophenol (372 mg) and 259 mg of 3-[N-(2,4-diacetoxy-3,3-dimethyl-1-oxobutyl)amino]propionic acid were reacted in the same manner as in Example 1 to obtain 255 mg of the title compound (yield: 39%).

Sources & evidence

ORD record: ord-a058bd1956724a7ab3ceb97f5e11439b
Source dataset: uspto-grants-1992_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05120738

Reaction notes

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