3-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid → HCID 67793921, compound

HRID 892899Notes

Reaction equation

HRID 892899 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][NH:6][C:7](=[O:25])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]/[CH:15]=[CH:16]\[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24].[CH3:26][C:27]1([CH3:43])[O:32][CH:31]([C:33]([NH:35][CH2:36][CH2:37][C:38](O)=[O:39])=[O:34])[C:30]([CH3:42])([CH3:41])[CH2:29][O:28]1>>[C:7]([NH:6][CH2:5][CH2:4][CH2:3][CH2:2][NH:1][C:38](=[O:39])[CH2:37][CH2:36][NH:35][C:33]([CH:31]1[C:30]([CH3:41])([CH3:42])[CH2:29][O:28][C:27]([CH3:43])([CH3:26])[O:32]1)=[O:34])(=[O:25])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]/[CH:15]=[CH:16]\[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

3

Reactant 2

HCID 189385173-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acidHCID 86745897HCID 86745897, compound

Product 1

HCID 67793921HCID 67793921, compoundYield 45%

Procedure

N-(4-Aminobutyl)oleamide (3.77 g) and 2.59 g of 3-[N-(2,2,5,5-tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid were reacted in the same manner as in Example 1 to obtain 2.66 g of the title compound (yield: 45%).

Sources & evidence

ORD record
ord-0e1103bf03244802a3dad5ef0b958b96
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

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