HCID 86745899, compound → HCID 86745898, compound

HRID 892900Notes

Reaction equation

HRID 892900 reaction equation
[C:1]([NH:20][CH2:21][CH2:22][CH2:23][CH2:24][NH:25][C:26](=[O:39])[CH2:27][CH2:28][NH:29][C:30](=[O:38])[CH:31]([OH:37])[C:32]([CH3:36])([CH3:35])[CH2:33][OH:34])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]>C(OC(=O)C)(=O)C>[C:1]([NH:20][CH2:21][CH2:22][CH2:23][CH2:24][NH:25][C:26](=[O:39])[CH2:27][CH2:28][NH:29][C:30](=[O:38])[CH:31]([O:37][C:33](=[O:34])[CH3:32])[C:32]([CH3:35])([CH3:36])[CH2:33][O:34][C:1](=[O:19])[CH3:2])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 1

HCID 86745899HCID 86745899, compound

Product 1

HCID 86745898HCID 86745898, compoundYield 164.2%

Reagents, catalysts & solvents 1

HCID 7918Acetic AnhydrideSolvent

Procedure

N-(4-Oleoylaminobutyl)-3-[N-(2,4-dihydroxy-3,3-dimethyl-1-oxobutyl)amino]propanamide (0.55 g) and 10 ml of acetic anhydride were reacted in the same manner as in Example 36 to obtain 0.52 g of the title compound (yield: 82%).

Sources & evidence

ORD record
ord-973ced8f379d4b4dbd91f267ad045c8c
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

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