3-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid → HCID 67795821, compound

HRID 892901Notes

Reaction equation

HRID 892901 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH:7][C:8](=[O:26])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]/[CH:16]=[CH:17]\[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25].[CH3:27][C:28]1([CH3:44])[O:33][CH:32]([C:34]([NH:36][CH2:37][CH2:38][C:39](O)=[O:40])=[O:35])[C:31]([CH3:43])([CH3:42])[CH2:30][O:29]1>>[C:8]([NH:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][NH:1][C:39](=[O:40])[CH2:38][CH2:37][NH:36][C:34]([CH:32]1[C:31]([CH3:42])([CH3:43])[CH2:30][O:29][C:28]([CH3:44])([CH3:27])[O:33]1)=[O:35])(=[O:26])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]/[CH:16]=[CH:17]\[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]

Participants

3

Reactant 2

HCID 189385173-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acidHCID 86745900HCID 86745900, compound

Product 1

HCID 67795821HCID 67795821, compoundYield 60%

Procedure

N-(5-Aminopentyl)oleamide (3.66 g) and 2.59 g of 3-[N-(2,2,5,5-tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid were reacted in the same manner as in Example 1 to obtain 3.64 g of the title compound (yield: 60%).

Sources & evidence

ORD record
ord-3f660e47a6a6446c97c87e1bd17e8e2f
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

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