3-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid → HCID 67793440, compound

HRID 892902Notes

Reaction equation

HRID 892902 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][NH:8][C:9](=[O:27])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]/[CH:17]=[CH:18]\[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26].[CH3:28][C:29]1([CH3:45])[O:34][CH:33]([C:35]([NH:37][CH2:38][CH2:39][C:40](O)=[O:41])=[O:36])[C:32]([CH3:44])([CH3:43])[CH2:31][O:30]1>>[C:9]([NH:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][NH:1][C:40](=[O:41])[CH2:39][CH2:38][NH:37][C:35]([CH:33]1[C:32]([CH3:43])([CH3:44])[CH2:31][O:30][C:29]([CH3:45])([CH3:28])[O:34]1)=[O:36])(=[O:27])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]/[CH:17]=[CH:18]\[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]

Participants

3

Reactant 2

HCID 189385173-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acidHCID 86745901HCID 86745901, compound

Product 1

HCID 67793440HCID 67793440, compoundYield 47%

Procedure

N-(6-Aminohexyl)oleamide (3.81 g) and 2.59 g of 3-[N-(2,2,5,5-tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid were reacted in the same manner as in Example 1 to obtain 2.92 g of the title compound (yield: 47%).

Sources & evidence

ORD record
ord-dde48842594244ee94feab5cde585460
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

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