3-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid → HCID 67794791, compound

HRID 892903Notes

Reaction equation

HRID 892903 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][NH:10][C:11](=[O:29])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]/[CH:19]=[CH:20]\[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28].[CH3:30][C:31]1([CH3:47])[O:36][CH:35]([C:37]([NH:39][CH2:40][CH2:41][C:42](O)=[O:43])=[O:38])[C:34]([CH3:46])([CH3:45])[CH2:33][O:32]1>>[C:11]([NH:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][NH:1][C:42](=[O:43])[CH2:41][CH2:40][NH:39][C:37]([CH:35]1[C:34]([CH3:45])([CH3:46])[CH2:33][O:32][C:31]([CH3:47])([CH3:30])[O:36]1)=[O:38])(=[O:29])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]/[CH:19]=[CH:20]\[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28]

Participants

3

Reactant 2

HCID 189385173-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acidHCID 86745902HCID 86745902, compound

Product 1

HCID 67794791HCID 67794791, compoundYield 21%

Procedure

N-(8-Aminooctyl)oleamide (4.08 9) and 2.59 g of 3-[N-(2,2,5,5-tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid were reacted in the same manner as in Example 1 to obtain 1.36 g of the title compound (yield: 21%).

Sources & evidence

ORD record
ord-4732884aeed54a8f942ecbc6eee7ff77
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

Loading…