9-Octadecenoic acid (9Z)-, 2-aminoethyl ester → HCID 67795113, compound

HRID 892904Notes

Reaction equation

HRID 892904 reaction equation
[C:1]([O:20][CH2:21][CH2:22][NH2:23])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[CH3:24][C:25]1([CH3:41])[O:30][CH:29]([C:31]([NH:33][CH2:34][CH2:35][C:36](O)=[O:37])=[O:32])[C:28]([CH3:40])([CH3:39])[CH2:27][O:26]1>>[C:1]([O:20][CH2:21][CH2:22][NH:23][C:36](=[O:37])[CH2:35][CH2:34][NH:33][C:31]([CH:29]1[C:28]([CH3:39])([CH3:40])[CH2:27][O:26][C:25]([CH3:41])([CH3:24])[O:30]1)=[O:32])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 64365999-Octadecenoic acid (9Z)-, 2-aminoethyl esterHCID 189385173-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid

Product 1

HCID 67795113HCID 67795113, compoundYield 31%

Procedure

2-Aminoethyl oleate (3.26 g) and 2.59 g of 3-[N-(2,2,5,5-tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid were reacted in the same manner as in Example 1 to obtain 1.75 g of the title compound (yield: 31%).

Sources & evidence

ORD record
ord-95ff61e252e944a6a1522cc76e54c421
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

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