N-(3-hydroxypropyl)hexadecanamide → HCID 19893384, compound

HRID 892911Notes

Reaction equation

HRID 892911 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][NH:5][C:6](=[O:22])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21].[CH3:23][C:24]1([CH3:40])[O:29][CH:28]([C:30]([NH:32][CH2:33][CH2:34][C:35](O)=[O:36])=[O:31])[C:27]([CH3:39])([CH3:38])[CH2:26][O:25]1>>[CH3:23][C:24]1([CH3:40])[O:29][CH:28]([C:30]([NH:32][CH2:33][CH2:34][C:35]([O:1][CH2:2][CH2:3][CH2:4][NH:5][C:6](=[O:22])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])=[O:36])=[O:31])[C:27]([CH3:39])([CH3:38])[CH2:26][O:25]1

Participants

3

Reactant 2

HCID 9922829N-(3-hydroxypropyl)hexadecanamideHCID 189385173-[N-(2,2,5,5-Tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid

Product 1

HCID 19893384HCID 19893384, compoundYield 99%

Procedure

N-(3-Hydroxypropyl)hexadecanamide (3.13 g) and 2.59 g of 3-[N-(2,2,5,5-tetramethyl-1,3-dioxane-4-carbonyl)amino]propionic acid were reacted in the same manner as in Example 15 to obtain 5.48 g of the title compound (yield: 99%)

Sources & evidence

ORD record
ord-a48b4199db6444fdb1b8b0adb58febf2
Source dataset
uspto-grants-1992_06
Patent number
US05120738

Reaction notes

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