HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perchloric Acid → HCID 14114898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perchloric Acid | HCID 24247 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 10921454 | HCID 10921454 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14114898 | HCID 14114898 | — |
Reaction Steps
A solution of 3-(2-(1,3-dioxolan-2-yl)ethyl)cyclohex-2-en-1-one (3.00 g), acetone (60.0 ml) and perchloric acid (3N, 10.0 ml) is stirred for 4 hr at 20°-25°. Aqueous saturated sodium bicarbonate (150 ml) is added and the mixture concentrated. Aqueous workup provides the title compound, IR (neat) 2950, 1720, 1666, 1257, 1194, 969, 732 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05120843 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-9aed00c903a644d295c8fb40437d47c1 |
| Source note | uspto-grants-1992_06 |