HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54540029, compound → 2,15-Hexadecanedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54540029 | HCID 54540029 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2,15-Hexadecanedione | HCID 458096 | — |
Reaction Steps
38 g of hexadeca-5,11-diene-2,15-dione (0.152 mole) were dissolved in 200 ml of ethyl acetate and hydrogenated at 50° C. under standard conditions using 1.9 g of 10% strength Pd/C. Recrystallization from petroleum ether gave 25.8 g of a 97% strength hexadecane-2,15-dione of melting point 80° C. The yield was thus 66% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05120880 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-2cc3c98048534693abe36f0205d17cdb |
| Source note | uspto-grants-1992_06 |