化工社化工社 化学情報印刷レポート · 研究参考用
1-Bromooctane → 3-Chloro-4-(octyloxy)benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Bromooctane | HCID 8140 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 3-Chlorosalicylic acid | HCID 74585 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 3-Chloro-4-(octyloxy)benzoic acid | HCID 18995369 | — |
反応手順
In 40 ml of ethanol were dissolved 10 g of 3-chlorohydroxybenzoic acid and 8 g of octyl bromide, and 40 ml a 2N aqueous solution of potassium hydroxide was added to the solution and the mixture was refluxed for 6 hours. The solution was made acidic and the precipitated crystal was recovered and recrystallized from an ethanol/water mixed solvent to obtain 9.5 g of 3-chloro-4-octyloxybenzoic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05124069 |
| 出典データセット | uspto-grants-1992_06 |
| ORD ID | ord-d0d499c5ee7b450e955cd8dec7963588 |
| 出典メモ | uspto-grants-1992_06 |