Ethyl 3-(2,4-dimethoxyphenyl)prop-2-enoate → HCID 14521157, compound

HRID 893412Notes

Reaction equation

HRID 893412 reaction equation
[CH3:1][O:2][C:3]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:4]=1[CH:5]=[CH:6][C:7]([O:9][CH2:10][CH3:11])=[O:8]>CO.[Pd]>[CH3:1][O:2][C:3]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:4]=1[CH2:5][CH2:6][C:7]([O:9][CH2:10][CH3:11])=[O:8]

Participants

4

Reactant 1

HCID 53804800Ethyl 3-(2,4-dimethoxyphenyl)prop-2-enoate

Product 1

HCID 14521157HCID 14521157, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 23938PalladiumSolvent

Procedure

100.2 g of ethyl 2,4-dimethoxycinnamate are dissolved in 400 ml of methanol and hydrogenated with palladium/charcoal under atmospheric pressure. The catalyst is filtered off with suction, and the filtrate is concentrated in vacuo.

Workup

  1. filtrationThe catalyst is filtered off with suction
  2. concentrationthe filtrate is concentrated in vacuo

Sources & evidence

ORD record
ord-41f624dd3f7d47a4841e4ce29292f9f8
Source dataset
uspto-grants-1992_06
Patent number
US05124478

Reaction notes

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