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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 893454Generated: October 30, 2026

Hydrochloric Acid → HCID 15341804, compound

https://huagongshe.com/reaction/893454

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantAmmonium ChlorideHCID 25517—
ReactantMethyl 2,4-dihydroxy-3-(prop-2-en-1-yl)benzoateHCID 13019279—
SolventPyrrolidineHCID 31268—
ProductHCID 15341804HCID 15341804—

Reaction Conditions

Temperature50 °C

Reaction Steps

Methyl 2,4-dihydroxy-3-(2-propenyl)benzoate (3.0 g) and a few crystals of ammonium chloride were added to 20 ml of pyrrolidine. The reaction mixture was heated to 50° C. and stirred overnight. The reaction mixture was neutralized with 10% hydrochloric acid and extracted with ethyl acetate. Concentration under vacuum to remove solvent gave the product as a light brown solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05124350
Source datasetuspto-grants-1992_06
ORD IDord-0a8a05d9e0444890b9bec1420b1de475
Source noteuspto-grants-1992_06