HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15341804, compound → HCID 15341825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15341804 | HCID 15341804 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15341825 | HCID 15341825 | 86% |
Reaction Steps
1-[2,4-dihydroxy-3-(2-propenyl)benzoyl]pyrrolidine (750 mg) in 2 ml ethanol was hydrogenated at room temperature and 5 psi for three hours using 4% Pd/C as catalyst. The solvent was removed under vacuum and the residue was chromatographed on silica gel using 50/50 ethyl acetate/hexane as eluant to give the product (650 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05124350 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-4942fc5a463c47c985e31aecb2cdf0c7 |
| Source note | uspto-grants-1992_06 |