Methyl vinyl ketone → HCID 53444549, compound

HRID 893530Notes

Reaction equation

HRID 893530 reaction equation
[CH:1]1[CH2:5][CH:4]=[CH:3][CH:2]=1.C([C:8]([CH3:10])=[O:9])=C.[CH3:11][CH2:12]CCCC>>[C:8]([C:2]12[CH2:1][CH:5]([CH2:11][CH2:12]1)[CH:4]=[CH:3]2)(=[O:9])[CH3:10]

Participants

4

Reactant 3

HCID 6570Methyl vinyl ketoneHCID 7612CyclopentadieneHCID 8058Hexane

Product 1

HCID 53444549HCID 53444549, compound

Procedure

In a 1-liter three-necked flask equipped with a Dimroth reflux condenser and a thermometer, 200 ml of cyclopentadiene and 200 ml of hexane were placed, cooled on water bath, and 200 ml of methyl vinyl ketone was added dropwise thereto while stirred over 30 minutes, and then stirred for 30 minutes, to obtain acetyl norbornene.

Workup

  1. customIn a 1-liter three-necked flask equipped with a Dimroth
  2. temperaturereflux condenser
  3. temperaturecooled on water bath
  4. stirringstirred for 30 minutes

Sources & evidence

ORD record
ord-22d1787abda74b56a6effa3b7e36fdc3
Source dataset
uspto-grants-1992_06
Patent number
US05126065

Reaction notes

Loading…