HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19890450, compound → HCID 18699345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19890450 | HCID 19890450 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18699345 | HCID 18699345 | 90.2% |
Reaction Steps
6-Benzyloxy 5-butoxy indole (4 g, 0.0135 mole) is hydrogenated under 50 atmospheres of hydrogen in a reactor with 40 ml of ethanol and 0.6 g 10% palladium on carbon for 3 hours. After filtration and evaporation of the solvent, the residue is recrystallized in a mixture of benzene-hexane to produce 5-butoxy 6-hydroxy indole (2.5 g, yield 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05126125 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-886432aa26414a84956e5430304dbab0 |
| Source note | uspto-grants-1992_06 |